ICI_118,551_hydrochloride_LCMS_16942_MedChemExpress

Data File D:\\AGLIENT 1260\\DATA\\20150709\\20150709 2015-07-09 09-04-13\\BIZ2015-708-DJL17.DSample Name: BIZ2015-708-DJL17=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 43Acq. Instrument : HY-LCMS-02 Location : P1-E-04Injection Date : 7/9/2015 12:08:40 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150709\\20150709 2015-07-09 09-04-13\\100-1500MS+3MIN_ 1.5(0.02%FA).MLast changed : 7/9/2015 11:40:35 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\BL10-80A(RP-HPLC).MLast changed : 7/9/2015 4:02:22 PM by Li Shan(LCMS-02) (modified after loading)Method Info : 10-80A,16MIN Catalog No : HY-13951 Batch#16942 A-RP-134 Additional Info : Peak(s) manually integrated DAD1 B, Sig=214,4 Ref=off (D:\\AGLIENT...0\\DATA\\20150709\\20150709 2015-07-09 09-04-13\\BIZ2015-708-DJL17.D) 1.760mAU1000800600400 2.39420000.511.5 2.00322.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.760 MM 0.0774 45.977 1171.97083 98.9951 2 2.003 MM 0.0473 51.23671 18.083 0.9314 3 2.394 MM 0.0476 4.04350 1.41596 0.0735 Totals : 5501.25775 1191.45161 ===================================================================== *** End of Report ***HY-LCMS-02 7/9/2015 4:02:23 PM Li Shan(LCMS-02)Page 1 of 1

Data File D:\\AGLIENT 1260\\DATA\\20150709\\20150709 2015-07-09 09-04-13\\BIZ2015-708-DJL17.DSample Name: BIZ2015-708-DJL17=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 43Acq. Instrument : HY-LCMS-02 Location : P1-E-04Injection Date : 7/9/2015 12:08:40 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150709\\20150709 2015-07-09 09-04-13\\100-1500MS+3MIN_ 1.5(0.02%FA).MLast changed : 7/9/2015 11:40:35 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\BL10-80A(RP-HPLC).MLast changed : 7/9/2015 4:03:19 PM by Li Shan(LCMS-02) (modified after loading)Method Info : 10-80A,16MIN Catalog No : HY-13951 Batch#16942 A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150709\\20150709 2015-07-09 09-04-13\\BIZ2015-708-DJL17.D) ES-API, Pos, Sca 1.766100000080000060000040000020000000.511.522.53min HY-LCMS-02 7/9/2015 4:03:20 PM Li Shan(LCMS-02)Page 1 of 2

Data File D:\\AGLIENT 1260\\DATA\\20150709\\20150709 2015-07-09 09-04-13\\BIZ2015-708-DJL17.DSample Name: BIZ2015-708-DJL17MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.766 9660559 279.20 I 278.20 I*MSD1 SPC, time=1.725:1.838 of D:\\AGLIENT 1260\\DATA\\20150709\\20150709 2015-07-09 09-04-13\\BIZ2015-708-DJL17.D ES-API100806040200100200300400500600700m/z 279.2 278.2Max: 785847 *** End of Report ***HY-LCMS-02 7/9/2015 4:03:20 PM Li Shan(LCMS-02)Page 2 of 2