MS Report from Instrument: LCMS-02 File ..0527 2017-05-27 08-34-16\\BIZ2017-527-WYQ4.D Tgt Mass (CHM): Injection Date : 27 May 17 12:31 pm +0800 Seq. Line : 51 Sample Name : BIZ2017-527-WYQ4 Location : P2-C-07 Acq. Operator : CLJ_701 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\chem32\\1\\DATA\\20170527\\20170527 2017-05-27 08-34-16\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\DATA\\20170527\\20170527 2017-05-27 08-34-16\\1-POS-3MIN.M Catalog No : HY-B1110A Batch#24719 A-RP-186 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C*DAD1 B, Sig=214,4 Ref=off 1.5501.0581.6631.7021..77868611.4521.4850.805mAU100050000.5*DAD1 C, Sig=2,4 Ref=off mAU15010050011.51.55022.53min*1.05811..66301..77863311.4521.4842.3650.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 704000030000200001000001.51.56622.53min*0.511.5 Ion 355.1, MSD1 355.1,Target Mass 3.1 +H Positive, EIC=3.8:355.8 1501005000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.53min22.53min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.81 0.02 6.11 4.09 0.17 ND 1.06 0.04 1179.20 527.34 33.07 ND 1.45 0.02 2.67 2.44 0.07 239 1.49 0.02 9.24 7.44 0.26 239 1.55 0.02 2320.00 1761.40 65.07 239 1.66 0.04 30.30 12.69 0.85 239 1.70 0.03 8.01 4. 0.22 239 1.77 0.02 4.68 4.55 0.13 239 1.79 0.02 5.38 4.06 0.15 239 Integration Results for DAD1 C, Sig=2,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.06 0.04 60.67 27.55 17.14 ND 1.45 0.08 0.40 0.40 0.11 239 1.48 0.05 0.60 0. 0.17 239 1.55 0.02 287.23 225.99 81.14 239 1. 0.03 0.66 0.79 0.19 239LCMS-02 5/27/2017 13:08:17 CLJ_701Page 1 of 3
MS Report from Instrument: LCMS-02 1.66 0.04 2.47 1.37 0.70 239 1.76 0.03 0.41 0.36 0.12 239 1.78 0.03 0.27 0.33 0.08 239 2.36 0.02 1.27 1.08 0.36 ND Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.57 0.11 385288.81 45749.38 100.00 239LCMS-02 5/27/2017 13:08:17 CLJ_701Page 2 of 3
MS Report from Instrument: LCMS-02Ret. Time: 1.57 <<<< POSITIVE SPECTRA >>>> ES-API Positive120001000080006000400020000200300400500600700m/z 240.1 239.1LCMS-02 5/27/2017 13:08:17 CLJ_701Page 3 of 3
