MS Report from Instrument: HY-LCMS-02 File ..M32\\1\\DATA\\20170503\\CPK\\CPK2017-503-06923.D Tgt Mass (EZX): 446.86 Injection Date : 3 May 17 5:32 pm +0800 Seq. Line : 0 Sample Name : CPK2017-503-06923 Location : P2-C-09 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No: HY-15180 Batch#06923 Easy-Access Method: '1-POS-3MIN' 446.86 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C*DAD1 B, Sig=214,4 Ref=off mAU6004000.57520000.7451.5141.3230.5*DAD1 C, Sig=2,4 Ref=off mAU150010000.482500011.3231.522.5min*1.4281.41.6061.6951.7341.8830.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 708000060000400002000001.51.47022.5min*0.511.5 Ion 447.86, MSD1 447.86,Target Mass 446.86 +H Positive, EIC=447.56:448.56 2001501005000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min22.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.57 0.03 8.51 5.56 0.97 157 0.74 0.04 2.13 0.99 0.24 ND 1.32 0.02 860.17 872.60 98.01 411 1.51 0.02 6.86 5.33 0.78 411 Integration Results for DAD1 C, Sig=2,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.48 0.02 2.75 0.03 0.14 ND 1.32 0.02 2013.80 2053.53 99.46 411 1.43 0.01 0.66 0.84 0.03 411 1.45 0.01 0.96 1.18 0.05 411 1.61 0.03 3.44 0.15 0.17 411 1.69 0.02 0.51 0.52 0.03 411 1.73 0.02 0.53 0.50 0.03 411 1.88 0.04 2.09 0.87 0.10 411HY-LCMS-02 5/4/2017 2:11:55 PM CLJ_701Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 1.47 <<<< POSITIVE SPECTRA >>>> ES-API Positive175001500012500100007500500025000200300400500600700800900m/z 206.1 411.1 412.1HY-LCMS-02 5/4/2017 2:11:55 PM CLJ_701Page 2 of 2
